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Powder metallurgy consisting of high-energy ball milling (HEBM) followed by con-solidation techniques is widely used to prep are multicomponent alloys and nanomaterials [39]. Advanced spark plasma sintering (SPS) has been widely used to improve the densi- fication rate of resultant bulk HEAs [40]. Recently, equiatomic non-Cantor AlCuSiFeZn HEA produced by HEBM and SPS exhibited a

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